FR4 is the most common grade dielectric material that is used in the fabrication of circuit boards. This material is incorporated in single-sided, double-sided, and multi-layered boards.

Here are a few qualities of FR4 materials that make them popular:

  • Wide range of operating temperature (50°C to 115°C)
  • Higher Tg value (about 180°C)
  • Offers decent mechanical properties to maintain board structure integrity
  • Cost friendly when compared to other materials

In this article, we will discuss the following points:

What does FR4 stand for?

FR4 laminates for PCB manufacturing

FR4 laminates

FR stands for flame retardant, and the number ‘4′ indicates woven glass-reinforced epoxy resin. The characteristics of FR4 vary significantly depending on the manufacturer, although it is commonly known for its mechanical strength and water resistance. This material performs as an insulator in PCBs by isolating adjacent copper planes while also providing overall mechanical strength.

What are the properties of FR4 substrate?

Flame retardant

Chemicals that are applied to materials to prevent or delay the spread of fire are known as flame retardants. FR4 substrates have excellent thermal, mechanical, and electrical properties making them a perfect choice for a wide range of electronic applications. Flame retardant laminates and prepregs are extremely versatile, adaptable to a variety of manufacturing procedures, and produce predictable results.

Good electrical properties

The electrical properties of a PCB material are critical for signal integrity and impedance considerations. They specify how fast an electrical signal propagates through the material and how much electrical charge it can retain in a given volume. The table below lists a few important electrical properties along with their typical values.

Electrical property Typical value
Dielectric constant (Dk) 5 at 1MHz
Electrical strength 800 to 1800volts/mil
Dissipation factor (Df) 0.009 at 1MHz
Surface resistivity (ρS) (Ohm/square unit) 105 to 1010

The given values can vary depending on the manufacturer. For example, FR4 has a dielectric constant that varies between 3.8 and 4.8 depending on the glass weaving style, thickness, and resin content.

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Low moisture absorption

Moisture absorption is the ability of a PCB material to resist water absorption when immersed in water. It is given by a percentage increase in the weight of a circuit board material due to water absorption under controlled conditions. FR4 materials offer a low moisture absorption of 0.10% when immersed in water for 24 hours.

FR4 material properties of various manufacturers

Name Manufacturer Glass transition temperature (Tg) Decomposition temperature (Td) Dielectric constant @ 10GHz Dissipation factor (Df) @ 10GHz Moisture absorption (%) Application area
FR370HR Isola 180 340 3.92 0.025 0.15 Normal speed, normal Loss
FR408HR Isola 200 360 3.63 0.0071 0.061 High speed, low loss
N4000-13 Nelco 210 350 3.6 0.009 0.1 Medium speed, low loss
N4800-20 Nelco 180 360 3.8 0.0075 0.07 High speed, low loss
VT-47 Ventec 170 340 4.27 0.016 0.12 Normal speed, normal loss
VT-901 Ventec 250 395 4.05 0.012 0.2 Normal speed, normal loss

Datasheet of Isola 370HR

Isola 370HR datasheet

Isola 370HR datasheet

Limitations of FR4 circuit board materials

FR4 has been used in the production of printed circuit boards for many years now. It’s inexpensive and provides adequate electrical insulation. However, when FR4 is used in high-speed applications the following problems may occur:

Insulating stability

Although FR4 is a great insulator, it has its limits when subjected to high power, voltage, or heat. If certain limits are exceeded, the materials’ insulating properties will deteriorate, and they will begin to conduct electricity instead. This causes circuit board failures.

Controlled impedance

FR4 does not offer uniform dielectric constant like high-speed board materials. As the frequency goes up the Dk varies. Dielectric constant tolerances for high-speed materials are less than 2%, whereas for FR4 it is up to 10%. Dk variations in FR4 impose challenges while maintaining impedance values. Hence, this material is not a preferred choice for controlled impedance boards.

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Signal losses

Signal loss is an important aspect of PCB design, particularly in high-frequency applications. FR4 isn’t the best material for these applications since it has a greater Df (dissipation factor) than high-frequency materials.

PCB material loss versus frequency for Rogers and FR4 material

PCB material loss versus frequency for Rogers and FR4 material. Image credit: EDN

FR4 has a Df of around 0.020, while most high-frequency laminates have a Df of around 0.004, which is a fourth of FR4’s Df. The smaller the Df, the lesser is the overall signal loss. One more drawback is that the Df of FR4 increases as the frequency of a signal increases. As a result, these PCBs suffer higher signal losses than a board built using a high-frequency laminate. The graph above plots frequency vs. loss per inch (dB) of FR4 and Rogers RO4350B (high-speed material). It clearly depicts that the FR4 material suffers a greater loss at high frequencies.

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High-Speed PCB Design Guide

Temperature stability

FR4 materials are not recommended for devices that are exposed to high temperatures. Also, these materials do not support lead-free soldering, this is because reflow temperatures for no-lead PCB assembly can reach up to 250 °C. This is significantly higher than the Tg of many FR4 versions.

Tips to select the right FR4 material

While choosing FR4 material, it’s critical to consider the thickness and other important characteristics of the laminate.

  • Avoid using thinner materials for circuit boards with grooves.

PCB with groove

PCB with groove

  • Choose a high-performance FR4 laminate if the operating temperature of the application exceeds 150 °C. These materials have better thermal performance and low expansion rates when compared to standard FR4 while retaining the same manufacturability. Isola 370HR is an example of high-performance FR4 material.
  • Select a dielectric material that offers a uniform dielectric constant (Dk) over a wide range of frequencies. The parasitic capacitance between a trace and its reference conductor, or between a trace and any other nearby conductors, will be affected by dielectric constant variations.

IPC-A-600 standard for FR4 materials

FR4 PCBs are made up of a square grid glass strands woven together. This sheet of woven glass is impregnated with epoxy resin and semi-cured to make a ply of prepreg. We discuss the IPC-A-600 or IPC-6012 standard related to base materials in the following section.

Standards related to the base material surface

Weave exposure

Weave exposure on FR4 materials

Weave exposure on FR4 materials

It is the state of the material in which unbroken woven cloth fibers on the surface are not entirely covered by resin as shown in the image above. Weave exposure is acceptable in all classes (class 1, 2, and, 3 boards) provided that the remaining space between conductors meets the minimum spacing requirement. For more about class 2 and class 3 boards, read IPC class 2 vs. class 3.

Weave texture

Weave texture on FR4 materials

Weave texture on FR4 materials

It is a condition in which the weave pattern is clearly visible on the surface but the fibers of woven cloth are fully covered in resin as seen in the image above. Weave texture is permissible in all classes, however, because of their similar appearances, it is commonly confused with weave exposure.

Standards related to base material subsurface

This section describes the subsurface conditions of laminated materials that are externally visible. Measling, crazing, delamination/blistering, and foreign materials are some of the most common subsurface base material conditions.

Measling

Measling on FR4 PCBs

Measling on FR4 materials

The presence of discrete white spots in the base material of a PCB is known as measling. Measling develops when the resin is not optimally applied to the board during the lamination process. Measles are permissible in all applications except for high-voltage products. However, excessive measling might decrease the board’s electrical and overall performance.

Crazing

Crazing on PCB laminates

Crazing on FR4 laminates

It is a phenomenon wherein a series of connected white spots or crosses appear in the base material indicating the separation of glass cloth fibers and connecting weave junctions.

Class 1 acceptability:

  • The space between conductive patterns should not be less than the minimum conductor spacing.

Class 2 and 3 acceptability:

  • Same as class 1 acceptability.
  • The distance between adjacent crazing patterns should not be more than 50% of the distance between adjacent conductive patterns.
  • Crazing at the board’s edge has no effect on the minimum distance between the board’s edge and the conductive pattern.

Delamination/Blister

Delamination blistering on PCB materials

Delamination/blistering on PCB materials

Any planar separation on a circuit board, such as between plies inside a base material, or between material and conductive foil is termed as delamination. Delamination characterized by localized swelling is termed as a blister.

Class 1 acceptability:

  • The area of the board affected by delamination does not exceed 1% of the total area.
  • The blister or delamination should be less than 25% of the distance between conductors.
  • Delamination should not be closer to the edge of the board.

Class 2 and 3 acceptability:

  • Same as class 1 acceptability.
  • The space between conductive patterns should not be less than the minimum conductor spacing.

Foreign materials

Foreign materials can be detected in raw (B-stage) laminate. They can be either conductive or non-conductive. Translucent particles trapped inside the PCB are permissible in all classes provided that the electrical and thermal properties of the board are not affected.

FR4 is the most commonly used material in PCB manufacturing. These boards are durable, water-resistant, and provide excellent insulation between copper layers, reducing interference and ensuring signal integrity. However, FR4 is not the greatest material to utilize in the boards operating at high frequencies or in harsh situations.

Let us know in the comments section if you have any queries related to FR board materials. We will be happy to help you out. To learn more about PCB materials check out our PCB material design guide. 

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This post was first published on: Sierra Circuits